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Random DO spikes in 500ml Ardagh Cans

  • 1.  Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-03-2024 12:46
    This message was posted by a user wishing to remain anonymous

    Friends, I have one of those problems we all relish solving from afar but wish we won't ever have in our Brewery!

    We are seeing an unpredictable DO result head to head on a 14-head canning line for 500ml Ardagh Widget Cans.

    In the past I've always found DO issues to be in purging settings, purging before sending beer over, dwell times or leaks. But I have never seen an issue I can't isolate to an area.

    The Data below is a 14-head assessment of DO using an Anton Paar Carbo QC with a 5-second head space flush before rinsing using zero oxygen nitrogen push gas and a timer for the rinse length. Before measurement, all samples were attemperated to 20 degrees and then shaken for 10 minutes on a wrist action shaker. Fill levels were consistently at or within 0.3% of the Nominal. 

    We have one seaming head and one nitrogen doser. Can moisture drip off the doser? I thought it would just freeze? 

    We are aware of air caught inside the widgets, but the table below surely should have some consistency in spite of that?

    Head number  DO levels (PPB)  on 03/07/2024 DO (PPB) set 2 03/07/24
    1 328 237
    2 530 274
    3 254 252
    4 235 218
    5 270 238
    6 490 316
    7 259 283
    8 216 323
    9 457 221
    10 509 458
    11 414 244
    12 288 446
    13 463 238
    14 214 241

    Any technical knowledge share on this would be fantastic, even just sharing an experience. Thank you very much. 



  • 2.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-05-2024 07:30
    Hi,
    All these DO???s are relatively high. Are you sure the filler/filling process is the root cause  of O2 pickup?
    Do you test the beer DO upstream of
    the filler (i.e.- beer before it enters the filler or in the BBT, at least.?)
    Do you have a pump feeding  the filler?
    If the DO is relatively low entering the filler then you can assume you???ve more or
    less isolated the issue to the  filler/filling process itself???otherwise, if possible, you need to work backwards sampling beer at various points to try and locate source of pickup.
    Side note..10 mins shaking seems excessive???I???m more familiar with SOP???s stipulating a few minutes.

     Best regards,


    Phil Leinhart, BSc
    First Key Consulting Inc. | Cooperstown, USA

    Tel: +1-607-547-2414 | Mob: +1-607-237-4468
    phil.leinhart@firstkey.com | www.firstkey.com

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  • 3.  RE: Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-05-2024 08:14
    This message was posted by a user wishing to remain anonymous

    All these DO???s are relatively high. - We are in control with BBT's and pre-filler levels. <20ppb. But thats not to say the pump is causing sporadic pull in of DO that hasnt been detected. Have you seen this before? 

    Are you sure the filler/filling process is the root cause of O2 pickup? We are getting <20 ppb on a pre-filler sampling point and in the Bright beer tank. 


    Do you test the beer DO upstream of
    the filler (i.e.- beer before it enters the filler or in the BBT, at least.?) - Yes - see above


    Do you have a pump feeding  the filler? Yes we do, and a theory exists that this is potentially a source - could you advise how to tell if it is? 

    If the DO is relatively low entering the filler then you can assume you???ve more or
    less isolated the issue to the  filler/filling process itself???otherwise, if possible, you need to work backwards sampling beer at various points to try and locate source of pickup. - We know the air in the Widgets cannot be completely purged and have confirmed this with another large US based Nitrogenated canning line. 


    Side note..10 mins shaking seems excessive???I???m more familiar with SOP???s stipulating a few minutes. - We have found this to be absolute as the headspace is so large including the widget space, it has proven the most accurate means for Measuring the N2 ppm in the can, which is critical to controlling can pressure. 




  • 4.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-05-2024 14:28

    Hi Anonymous,

    I agree with Phil that these DOs are quite high, however I have NO experience with nitrogenated products so not sure if these values are considered normal. To provide perspective, we run a 16:4 rotary filler and seamer with all carbonated beer (2.5-2.85v/v depending on brand). Our TPO upper limit is 40ppb with operating ranges for 25-40ppb. 

    There are a lot of variables in controlling O2 pickup during filling and providing some more info would help track down some root causes. 

    • I assume with 14 valves this is a counter pressure rotary line, but would you confirm? 
    • What are your unshaken can values? These would let you know if the ingress is during the transfer of beer to the can (pump, bowl, etc) or after. If these are high, then perhaps it is the pump - have seals been changed regularly? 
    • You did not specify, but are these just the shaken can values or are they plugged into the V/U equation to estimate package TPO? Regardless, in my experience excessively high and variable shaken DO or TPO tend to be related to after fill operations: conveyor transitions (shaking cans), FOB formation, dwell time b/t filler and seamer, bubble breaker (pressure + flow), and undercover gassing (pressure + flow). 
      • Don't underestimate the value of a steady transfer of cans off of the filling carousel and into the seamer. If any beer is shaking out, O2 is coming in.
    • Is the beer carbonated or nitrogenated prior to filling or are you filling still and relying on the liquid N2? If the latter, how do you normally control headspace O2 during post fill and seaming? Are you using cover gas? If so, is it CO2 or N2? Could purity have changed?

    Any other relevant info would be great. There are a lot of canning experts on this forum who will all likely have some intel. 



    ------------------------------
    Campbell Morrissy, PhD
    Director of Brewery Operations
    pFriem Family Brewers
    ------------------------------



  • 5.  RE: Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-06-2024 11:42
    This message was posted by a user wishing to remain anonymous

    • I assume with 14 valves this is a counter pressure rotary line, but would you confirm? Correct
    • What are your unshaken can values? These would let you know if the ingress is during the transfer of beer to the can (pump, bowl, etc) or after. If these are high, then perhaps it is the pump - have seals been changed regularly? Yes, the values vary but we lose 100 ppb in the Pasteurisation process through assumed oxidation, these cans in the data table are unpasteurised cans. To my knowledge no seals have been replaced since commissioning 14 months ago. Would you recommend seals change annually? Regarding the Shaking step, No, we haven't done a head check with unshaken cans. 
    • You did not specify, but are these just the shaken can values or are they plugged into the V/U equation to estimate package TPO? No, the extended shake just helps us determine what levels of N2 the doser is giving us. 
    • Regardless, in my experience excessively high and variable shaken DO or TPO tend to be related to after fill operations: conveyor transitions (shaking cans), FOB formation, dwell time b/t filler and seamer, bubble breaker (pressure + flow), and undercover gassing (pressure + flow). 
      • Don't underestimate the value of a steady transfer of cans off of the filling carousel and into the seamer. If any beer is shaking out, O2 is coming in. - We have a CO2 tunnel that mitigates pickup in the dwell time. 
    • Is the beer carbonated or nitrogenated prior to filling or are you filling still and relying on the liquid N2? If the latter, how do you normally control headspace O2 during post fill and seaming? With the CO2 tunnel.
    • Are you using cover gas? If so, is it CO2 or N2? Could purity have changed? Cans are Dosed with liquid Nitrogen. We havent turned off the doser to isolate if this N2 doser is the source yet as the Supplier certificates show some DO in the Liquid itself <1ppm. 



  • 6.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-05-2024 14:29
      |   view attached

    So I took a stab at graphing some of the data (see attached, and picture), and I'm not sure I see a compelling case for a difference DO by filler head with the notable exception of head number 10. I also think there might be a sampling/measurement technique misstep when measuring the DO, because the data are pretty noisy overall and I don't doubt that there is an issue somewhere.

    A cause of filler head DO pickup I have seen before is the result of trapped cleaning chemicals and gas bubbles around o-rings and seals that had become unseated, jammed, or just worn, leading to voids where matter could accumulate. If you haven't done a filler teardown already (and I suspect you may have), it's probably time to do so and replace as many seals as you can justify (as they are usually much cheaper to see to now than continuing to worry and should delay the next teardown).

    Hope that helps.

    Cheers,

    -Matt





    ------------------------------
    Matt Philip (WeCanDrinkTogether)
    Severn ON
    (519) 588-3242
    ------------------------------

    Attachment(s)



  • 7.  RE: Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-06-2024 11:41
    This message was posted by a user wishing to remain anonymous

    Really appreciate your input Matt. Regarding the Noisy data thats the main source of my frustration as the CO2 and N2 levels in these samples were predictable and steady values - particularly CO2 but also N2 with a standard deviation of about 4ppm. 




  • 8.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-06-2024 18:36

    Pumps can be weak points regarding oxygen ingress typically when seals fail due to various reasons such as running dry, etc. A way to determine is to test the beer DO on the discharge side of the pump, if possible. If the reading is significantly higher at this point relative to the suction side of the pump, such as in the BBT, then the pump could be a source of pickup. It is also important to ensure all connections, clamps, fittings, etc are not potential sources of O2 pickup. All this said, you mention you are getting <20 ppb at the pre-filler sampling point. Assuming this sampling point is downstream of the pump and just before the beer enters the filler, it does point to the filler/filling process being the likely source of your issue and following the recommendations of others on this thread would be a good plan of action. I would also add that there is a great MBAA podcast regarding small scale canning. It is very practical and reviews the various quality control points and operating parameters to ensure low DO pickup.

    Best regards,



    ------------------------------
    Phil Leinhart
    First Key Consulting
    Cooperstown NY
    (607) 237-4468
    ------------------------------



  • 9.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-05-2024 14:27

    Hi Fellow Brewer,

    Probably air pick up from the Head Space.

    Try manipulating your Undercover gasser and bubble breaker. Also level of beer carbonation. 

    I've even seen a jetter on a bottle filler work on can fillers.

    Good Luck

    Dan Carey 

    New Glarus Brewing 



    ------------------------------
    Daniel Carey
    Brewmaster
    New Glarus Brewing Company
    New Glarus WI
    (608) 527-5850
    ------------------------------



  • 10.  RE: Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-06-2024 10:56
    This message was posted by a user wishing to remain anonymous

    In terms of manipulating the Jetter or Tunnel have you seen it carried out anywhere that the Tunnel has a stone feed so the gas sparges evenly across the top of the tunnel? At the moment its just 4 outlets through 12mm vents with a perspex covering on each side. 




  • 11.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-07-2024 18:51

    Hi Anonymous

     

    Sorry, I'm not familiar with such a design so I can't offer specific guidance. I can only point you in the right direction. Solving these types of issues is like detective work and "every crime is unique"

     

    In my experience, the largest contributor to Can TPO is, by far, from the head space. How you Inert Gas Purge head space just before applying the End is critical. Cans are especially vulnerable, compared to a Long Neck Bottle, due to the large surface area exposed to atmosphere. Without a gentle purge before lid (or as the homebrewers say, "Cap on foam"), it's easy to exceed a 1,000 ppb contribution!

     

    I suggest you speak with your Can Filler Vendor as they should have suggestions. Also, visit a brewery that you respect in your area and ask to see how a properly adjusted seamer is set up. Small tweaks can have a huge impact.

     

    Some basics for TPO management.

    1. Is your DO meter calibrated? When hooked up to an active fermenter, it should read near 0 ppb.
    2. Is the meter accurate? We use a Trace Verifier for this purpose. The team at Hach came up with a nice way to inject a given amount of air into a can so you can check span.
    3. Once you trust your DO meter, start with the Bright Beer Tank. You should be able to achieve << 20 ppb
    4. Check DO in your Filler Bowl. It should be the same, or close to the same, as the BBT if tanks/hoses were purged well and pump seal is good (and your CO2 has low DO).
    5. How much DO was picked up across the Filler? Check TPO ASAP off the Seamer without shaking. If you find the high values you have been seeing, it could indicate improper can purge or fill. But be aware, high Head Space DO will "drag up" the beer DO
    6. Do your normal check with Rest and Shake. If previous tests were moderate but high here, it might indicate head space pick up.

     

    A TPO tester that separately reports Beer DO, Head Space DO and TPO would help. Is there a brewery close to you that has one? If you could get a few cans to then quickly before the oxygen reaches equilibrium (10's of minutes not hours), you could really narrow down the source.

     

    Good Luck

    Dan Carey

    New Glarus Brewing

     






  • 12.  RE: Random DO spikes in 500ml Ardagh Cans

    This message was posted by a user wishing to remain anonymous
    Posted 07-10-2024 06:54
    This message was posted by a user wishing to remain anonymous

    Hi all, two separate items to ask about here. 

    1. Bowl level - 50% - If you go higher than 50% I assume the impact of CO2 pickup in the bowl is slowed down? More over the volume of liquid helps slow down the speed of the temperature rise? 
    2. Fobbing - if the temperature at filling varies, so too does your level of fobbing in the filling / dwell time?

    All connected to solving the DO issue 

    Thanks




  • 13.  RE: Random DO spikes in 500ml Ardagh Cans

    Posted 07-10-2024 14:46

    Anonymous

    Dan has given you very good advice. I want to emphasize his head space comments. More head space = higher DOs. 

    Bowl level - you should follow the manufacturer's recommendation for bowl level. We run our bowls (bottle and can) at 45% and no higher than 50%. The beer is in the bowl for such a short amount of time that there should be little or no CO2 pickup. We run ours at 30 PSI and we never see any CO2 pickup.

    DO - Can fillers that I've seen, other than high end machines, vent can gas to the bowl. If your can purge is inadequate then you are dumping a bunch of O2 into the bowl. Those machines should have a bowl purge so you should check that to be sure that your bowl purge is adequate. 

    Consider picking three heads from each run and pull cans from those heads three different times during the run and compare the DOs. This will allow you to check every head within a five run block. We use this method to identify any soft parts that are beginning to fail.

    Final thought – Reducing your head space reduces DO.

    KT



    ------------------------------
    Kent Taylor
    Blackstone Brewing Co
    Nashville TN
    (615) 327-8111
    ------------------------------