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  • 1.  Nitrogen Purity Requirements/Residual O2 levels for Different Brewery Applications

    Posted 12-18-2024 13:58

    Hi All, We are considering purchasing a Nitrogen Generator to reduce our brewery CO2 requirements.  Obviously N2 can be used for different applications around the production area (purging tanks, pushing beer, purging cans and kegs).  However I am having a hard time pinning down an exact N2 Purity percentage for best practice. 

    The issue is the higher the Nitrogen Purity, the larger the Nitrogen Generator needs to be for the same flowrate and also the higher compressed air requirements it has.  Meaning the higher the purity, the larger and more expensive the set up will be. 

    We obviously don't want to spend more than necessary, but don't want to get too small of a unit either,  so I was just wondering if anyone has any practical real world experience with what nitrogen purity worked for them and in what applications.  

    Any information would be greatly appreciated! 



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    Daniel MacKinnon
    Co-Owner
    MacKinnon Brothers Brewing
    Bath ON
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  • 2.  RE: Nitrogen Purity Requirements/Residual O2 levels for Different Brewery Applications

    Posted 12-19-2024 13:49

    Hi Daniel, 

    From my experience with brewery applications such as water de-aeration or nitrogenation, the recommended purity spec for the N2 is >/=99.99%.

    I hope that helps!

    Best regards, 

    Mike 

     



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    Michael Miziorko
    Product Manager-Brewing Technology
    Gusmer Enterprises
    Saint Paul MN
    (612) 368-9886
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  • 3.  RE: Nitrogen Purity Requirements/Residual O2 levels for Different Brewery Applications

    Posted 12-19-2024 17:51

    Wow, N2 generators are so hot right now! Just an FYI there is a similar thread about purging BTs with generated N2.

    We spent a lot of time looking at this balance when choosing, installing, and tuning in our generator. We were back and forth deciding between a Holtec and Parker unit and one of the reasons we went with Holtec was that it was rated for the the same purity at a lower inlet air pressure (flowrates were the same). This allowed us to install without upgrading our compressed air plant. 

    Despite what some vendors will claim, we found that for many processes, we did need to generate high purity N2 (99.99 - 99.999%) to mimic the performance of CO2*. You also may find that your unique process and equipment requires a purity that doesn't match another brewery's requirements. The nice thing is that most generators will allow you to modulate the operating conditions** in order to achieve your target purity. Our is monitored via an O2 sensor with thresholds that we can plug into to set alarm conditions. Our goal is N2 removal so there is probably trace CO2 and Argon in the N2 stream that we wrap into that purity %. 

    The area we look at most and the main driver behind the install is N2 at the can seamer. We run N2 exclusively on the bubble breaker and under lid gassing star. Speaking to another well respected brewery, we were told that we should have 99.995% or better to keep TPO in spec. We've confirmed those findings and further found anything lower than 99.99% produces a >10 ppb penalty. Depending on your internal specifications for TPO that may be acceptable if you can reduce your operating costs on the generator. For us, we run a pretty low TPO spec and want to maintain/improve any place we can. If you have the ability to modulate flow, and thus N2 purity, you can dial it in to provide the balance that works for your brewery. We also use that purity for BT purges and adjunct additions into FVs or BTs - but that is based on convenience as the can seamer is the main user in the brewery and not measurements in those areas. 

    I'd be happy to speak to our experience if you have other questions. 

    *we didn't regularly measure our purchased CO2 purity to audit the suppliers claims. Just FYI. 

    **a major driver is the ambient temperature of the room the generator is in. While we knew that this would have an impact we were surprised by how noticeable it was We saw a 0.005-0.01% purity penalty when running in a non-climate controlled room during the summer (+50-100ppm O2). We've since ducted the air compressors outside, dropping the temp of the room by 25°F in the summer and immediately saw an improvement in performance. Bonus, we can duct the air back into the room in the winter to keep it at a nice temp. I know other folks will have HVAC dedicated for this purpose. 



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    Campbell Morrissy, PhD
    Director of Brewery Operations
    pFriem Family Brewers

    Campbell Morrissy, PhD
    Director of Brewery Operations
    pFriem Family Brewers

    MBAA NTC - Committee Chair
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  • 4.  RE: Nitrogen Purity Requirements/Residual O2 levels for Different Brewery Applications

    Posted 01-06-2025 10:32

    Hi Campbell, 

    What method was used to measure the purity of the Gas? Our N2 generator engineer said the Anton Paar Carbo QC did not measure DO in gas form, but yet high purity N2 is used in gas form to blank check the DO measurement. Based on this I couldn't understand how our result of N2 gas from the generator was not deemed valid by the Supplier. 



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    Sean Matthews
    Quality Manager
    Forged Irish Stout
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  • 5.  RE: Nitrogen Purity Requirements/Residual O2 levels for Different Brewery Applications

    Posted 01-08-2025 14:20

    I realized I sent this as a direct message instead of a reply to the thread and thought it might be useful to share publicly. 

    We have an integrated O2 sensor (electrochemical) on our Holtec generator that reads out in ppm and displays on the HMI. We operate under the assumption that other atmospheric gasses (CO2/Ar) are minimal and mostly removed in the same mechanism in the generator, and thus use that to O2 ppm to calculate N2 %. At least CO2 is a smaller molecule than N2 and should be retained in the media. Given these trace gasses don't change the impact of our process that works for us. So yes, technically our gas % may not be truly 99.995% N2 but ultimately we do know our O2 concentrations are where we need them. From my understanding Parker generators also provide O2 sensors. 

    We do use a standard DO instrument to measure tank purges. We use our Orbisphere 3100 in the gas phase and I have had good success with this method with both the 3100 and AP cBox for the past 8-9 years. I know that this is not considered an accurate measurement of O2 in the gas phase, but we find it to be repeatable and thus suitable for our purposes. I don't quite understand why these aren't considered accurate but this method works fine to audit tanks. 

    Hopefully that helps. 



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    Campbell Morrissy, PhD
    Director of Brewery Operations
    pFriem Family Brewers

    MBAA NTC - Committee Chair
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